Publications

PUBLICATIONS ON THE MISOTOP PROJECT

• “Induction-heated ball-milling: a promising asset for mechanochemical reactions“
  G. Félix*, N. Fabrègue, C. Leroy, T.-X. Métro, C.-H. Chen, D. Laurencin*, ChemRxiv 2022, doi : 10.26434/chemrxiv-2022-2326c

• “Fast and cost-efficient approaches for ¹⁷O-isotopic labeling of carboxylic groups in biomolecules: from free amino acids to peptide chains“
  J. Špačková*, I. Goldberga, R. Yadav, G. Cazals, A. Lebrun, P. Verdié, T.-X. Métro*, D. Laurencin*, Chem. Eur. J. 2023, 29, e202203.

• “Oxygen-17 solid state NMR as a valuable tool for deciphering reaction mechanisms in mechanochemistry: the case study on the enrichment of hydrated Ca-pyrophosphate biominerals“
  I. Goldberga*, N. D. Jensen, C. Combes, F. Mentink-Vigier, X. Wang, I. Hung, Z. Gan, J. Trébosc, T.-X. Métro, C. Bonhomme, C. Gervais, D. Laurencin*, Faraday Discuss, 2023, 241, 250-265.

• “Operando acoustic analysis: a valuable method for investigating reaction mechanisms in mechanochemistry“
  C. Leroy*, S. Mittelette, G. Félix, N. Fabregue, J. Špačková, P. Gaveau, T.-X. Métro, D. Laurencin*, Chem. Sci., 2022, 13, 6328-6334.

• “First direct insight into the local environment and dynamics of water molecules in the whewellite mineral phase: mechanochemical isotopic enrichment and high-resolution ¹⁷O and ²H NMR analyses“
  I. Goldberga*, N. Patris, C.-H. Chen, E. Thomassot, J. Trébosc, I. Hung, Z. Gan, D. Berthomieu, T.-X. Métro, C. Bonhomme, C. Gervais, D. Laurencin*, J. Phys. Chem. C, 2022, 126, 29, 12044-12059.

• “From operando Raman mechanochemistry to “NMR crystallography”: understanding the structures and interconversion of Zn-terephthalate networks using selective ¹⁷O-labelling“
  C. Leroy*, T.-X. Métro, I. Hung, Z. Gan, C. Gervais, D. Laurencin*, Chem. Mater., 2022, 34, 5, 2292-2312.

• “Cost-efficient and user-friendly ¹⁸O/¹⁷O labeling procedures of fatty acids using mechanochemistry“
  J. Špačková, C. Fabra, G. Cazals, M. Hubert-Roux, I. Schmitz-Afonso, I. Goldberga, D. Berthomieu, A. Lebrun, T.-X. Métro*, D. Laurencin*, Chem. Commun., 2021,57, 6812-6815.

• “Labeling and Probing the Silica Surface Using Mechanochemistry and ¹⁷O NMR Spectroscopy“
  C.-H. Chen*, F. Mentink-Vigier, J. Trébosc, I. Goldberga, P. Gaveau, E. Thomassot, D. Iuga, Mark E. Smith, K. Chen, Z. Gan, N. Fabregue, T.-X. Métro, B. Alonso*, D. Laurencin*, Chem. Eur. J, 2021, 27, 12574-12588.

• “Looking into the dynamics of molecular crystals of ibuprofen and terephthalic acid using ¹⁷O and ²H NMR analyses“
  C.-H. Chen, I. Goldberga, P. Gaveau, S. Mittelette, J. Špačková, C. Mullen, I. Petit, T-X. Métro, B. Alonso, C. Gervais, D. Laurencin*, Magnetic Resonance in Chemistry. 2021, 59, 975-990.

• “Unveiling the structure and reactivity of fatty-acid based (nano)materials thanks to efficient and scalable ¹⁷O and ¹⁸O-isotopic labeling schemes”
  J. Špačková, C. Fabra, S. Mittelette, E. Gaillard, C.-H. Chen, G. Cazals, A. Lebrun, S. Sene, D. Berthomieu, K. Chen, Z. Gan, C. Gervais, T-X. Métro*, D. Laurencin*, J. Am. Chem. Soc. 2020, 142, 21068.

• “Direct ¹⁷O-isotopic labeling of oxides using mechanochemistry”
  C.-H. Chen, E. Gaillard, F. Mentink-Vigier, K. Chen, Z. Gan, P. Gaveau, B. Rebière, R. Berthelot, P. Florian, C. Bonhomme, Mark E. Smith, T.-X. Métro, B. Alonso, D. Laurencin, Inorg. Chem. 2020, 18, 13080. Cover.

• “L’enrichissement isotopique en oxygène-17 grâce à la mécanochimie : vers de nouvelles opportunités pour la RMN ¹⁷O
  D. Laurencin, T.-X. Métro, Fiche “Un point sur n°57”, Actualité Chimique, 2018, 430-431, 127-128.

• “Unleashing the potential of ¹⁷O NMR using mechanochemistry”
  T.-X. Métro, C. Gervais, A. Martinez, C. Bonhomme, D. Laurencin, Angew. Chem. 2017, 56, 6803. Cover.